Some new cyanopyridine derivatives have been synthesized and characterization of the synthesized compounds was done by IR, NMR and mass spectral data. The thermal properties of these compounds were studied by thermogravimetry. The thermal stability, melting temperature and some kinetic parameters such as energy of activation, frequency factor, order of reaction and entropy of activation were evaluated from thermograms. The degradation is single step process for some compounds whereas for others, it is multi step process.
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